Cryo-EM is used to preserve and characterize cycled positive electrodes. Under regular cycling conditions, there isn't an intimate coating layer like CEI.A small electrical short can cause a stable conformal CEI to form in place. The conformal CEI's chemistry is revealed by EELS and cryo-(S)TEM.
It has been assumed that the intimate coating layer generated on the positive electrode, known as cathode electrolyte interphase (CEI), is crucial. However, there are still numerous questions about CEI. This results from the absence of useful instruments to evaluate the chemical and structural characteristics of these delicate interphases at the nanoscale. Here, using cryogenic electron microscopy, we establish a methodology to maintain the natural condition and directly see the interface on the positive electrode.
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