Answer: See image attached!
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The researcher may first weight the beaker with water and then start to heat the water to a constant temperature, for example 30 °C and then start adding salt and stirring. He should add salt slowly until solid salt starts to become visible and the solution starts becoming cloudy. When this happens, he should quickly weigh the beaker. The increase in mass is the mass of salt dissolved at that temperature.
The procedure is then repeated but at an increased temperature until 5-6 temperatures have been tested.
Answer:
(FeSCN⁺²) = 0.11 mM
Explanation:
Fe ( NO3)3 (aq) [0.200M] + KSCN (aq) [ 0.002M] ⇒ FeSCN+2
M (Fe(NO₃)₃ = 0.200 M
V (Fe(NO₃)₃ = 10.63 mL
n (Fe(NO₃)₃ = 0.200*10.63 = 2.126 mmol
M (KSCN) = 0.00200 M
V (KSCN) = 1.42 mL
n (KSCN) = 0.00200 * 1.42 = 0.00284 mmol
Total volume = V (Fe(NO₃)₃ + V (KSCN)
= 10.63 + 1.42
= 12.05 mL
Limiting reactant = KSCN
So,
FeSCN⁺² = 0.00284 mmol
M (FeSCN⁺²) = 0.00284/12.05
= 0.000236 M
Excess reactant = (Fe(NO₃)₃
n(Fe(NO₃)₃ = 2.126 mmol - 0.00284 mmol
=2.123 mmol
For standard 2:
n (FeSCN⁺²) = 0.000236 * 4.63
=0.00109
V(standard 2) = 4.63 + 5.17
= 9.8 mL
M (FeSCN⁺²) = 0.00109/9.8
= 0.000111 M = 0.11 mM
Therefore, (FeSCN⁺²) = 0.11 mM